... experiment is as following: 100 mL round bottom flask, stir bar, water condenser, hot plate, UV light, Pasteur pipet, ice bath, separatory funnel, rotary evaporator, evaporating dish, cotton for filtering, and UV-vis spectrometer. Quinn 2 The chemicals required are: 0.1 g. of H2TTP made previously, 20 mL N,N-dimethylformamide, 0.16 g. hydrated copper acetate, distilled water, 75 mL dichloromethane, hexane, toluene, ethyl acetate, dichloromethane, and acetone for TLC plates. Procedure 1. Measure out 0.1 g. of the H2TTP made previously into a 100 mL round bottom flask with a stir bar. 2. Add 20 mL of N,N-dimethylformamide (a bright blue powder) and let the solution stir. 3. Add 0.16 g. of hydrated copper (II) acetate, cover with a water condenser and allow to reflux for 30 minutes. 4. Spot the solution on a TLC plate and check with UV light to see if there is any red on or around the spot. Add additional ...

See this essay or coursework document in full right now